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Some notes on Carbon HPHT

Some notes on Carbon HPHT Page of 35 Some notes on Carbon HPHT Text size:minus plus Restore normal size   Mail page  Print this page
230                                      EXPERIMENTS ON THE
or without sulphur, were first heated and well boiled in the carbon crucible at atmospheric pressure, and after cooling transferred to the vacuum furnace and re-heated by resistance under X-ray vacuum; violent ebullition occurred owing to the liberation of occluded gases, and many iron spherules were ejected, which cooled by radiation and conduction where they fell; diamond was found in these, which burnt in oxygen, but no diamond was ever found in the ingot remaining in the crucible.
It occurred to us to try the effect of great mechanical pressure accom­panied by heat upon small particles and powders, the interstices being exhausted to a high vacuum.
Several experiments were made in the press under a mass pressure of 3000 atmospheres.
A layer of cast-iron turnings resting on a layer of carborundum grit, the exhaustion being effected through a hole in the side of the mould covered by a perforated steel plate within the layer of grit, heat was applied as usual by a central carbon rod.
Analysis yielded some thin crystal plates from the grit which had lain in the line between the cast iron and the suction outlet at the grid, and also from the layer of grit which had lain against the cast-iron turnings which had become heated but not melted by the central carbon rod.
To ascertain the cause of the occurrence of these plates, experiments were made, without bulk pressure, on the concentrated action of the gases given off from cast-iron turnings heated up to a good red, and drawn by a high-vacuum pump through carborundum grit placed in a silica tube
Some notes on Carbon HPHT Page of 35 Some notes on Carbon HPHT
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Parsons. Synthetic Diamond.
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